Production of light berries black pepper essential oil on pilot scale by hydrodistillation

MEng. Do Dinh Nhat

Black  pepper  (Piper  nigrum  L.)  is  a  tropical  crop  with  extensive  medicinal  potential  in ethnomedicine  and nutraceutical  applications.  In  this  study,  the  hydro-distillation  method  was  employed  in  the  extraction  of  essential  oil  from light  berries  black  pepper  (300g/L).  Extraction  parameters  such  as  time,  temperature,  and  the  ratio  of  solid/solvent  were optimized. The quantitative analyses of the essential oils were performed by GC/MS. The optimum yield was achieved up to 2.383%  when  the  extract  conditions  were  set  up  at  material-water  ratio  of  1:12,5  for  180  minutes  under  the  extraction temperature of 130 0C. The result of GC-MS showed that 3-Carene (23.27%), D-limonene (14.74%) and β-caryophyllene (28.28%) were  presented as  major components.The  results of this study on the  pilot scale  could be  useful  for technology transfer, which mightbecome the solution to shorten the gap between research and production.

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